The effect of various factors on the yield of 2,3,3–triiode propene–2–ol–1

Abstract

A triode derivative of propargyl alcohol has been synthesized, and the effects of catalyst concentration, time and temperature on the synthesis process have been studied. Various concentrations of alkalis (5,0–30,0 mass. %) have been used as catalysts. It has been found that 2,3,3–triode propene–2–ol–1 has a higher yield when the concentration of the catalyst NaOH is 15%. The effect of time duration (1–5 hours) on product productivity has also been studied. Product yield has been found to be high for 3 hours. In addition, the effect of temperature on the product’s productivity has also been studied at intervals of (10–60°C). It has been found that the yield of 2,3,3–triiodpropen–2–ol–1 was high in 3 hours at 20°C. The structure of the synthesized substance was studied and confirmed by the methods of IR– and NMR–spectroscopic analysis.