The effect of stress state and He concentration on the dislocation loop evolution in Ni superalloy irradiated by Ni+ & He+ dual-beam ions: In-situ TEM observation and MD simulations

Abstract

In-situ TEM observation was conducted during Ni+&He+dual-beam irradiation to monitor the evolution of dislocation loops accompanied by He bubbles in the Ni-based alloy GH3535. Two distinct evolutions of dislocation loops, driven by residual stresses, were observed within the monitored grains. Hence, molecular dynamics (MD) simulations were employed to reveal the effects of stress magnitude and direction on loop evolution, including size, number density, type and variation. The simulations revealed that the presence of compressive stress reduced the formation energy of perfect dislocation loops, thus promoting their formation. Stress state was found to influence the preferential orientation of the loops, and compressive stress resulted in a decreased number density of dislocation loops but an increase in their size. This establishes a clear relationship between stress state and magnitude and the evolution of dislocation loops during ion beam irradiation. Additionally, the nature and characteristics of dislocation loops were quantified to explore the effects of He concentrations on their evolution. The higher He concentration not only promotes the nucleation of dislocation loops, leading to their higher number density, but also facilitates the unfaulting evolution by increasing the stacking fault energy (SFE). Moreover, the accumulation of He in the lower-He-concentration sample led to the growth of dislocation loops in multiple stages, explaining their nearly identical average sizes when compared to the higher-He-concentration sample.