Abstract
An acidimetric double titration method for the determination of Grignard compound has been developed which compensates for the free basicity present in the solution. The active Grignard compound present in solution was reacted with carbon tetrachloride to produce neutral magnesium chloride, allowing free basic magnesium to be subsequently determined by titration. A correction was thus applied to an acidimetric titration on the original Grignard solution to give a reliable determination of the concentration of active Grignard compound in solution.
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