Abstract
The gassing rate, , of powder samples, made by the chemical oxidation of , was measured in gassing pipettes. The mean of 52 samples at 200 hr was 23.0 µl/day/g. Gassing rates at different times and in different solutions, respectively, are correlated. increased with increasing concentration, temperature, and pelletizing pressure, and with ball milling, of samples made in the presence of transition elements (added as compounds) were, in general, larger than of samples with nontransition elements. The effect of Co and Ni is especially catastrophic. Pb suppressed of highly gassing samples regardless of the method of addition.
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