Abstract
The crystal of l-arginine monohydrobromide monohydrate belong to space group P21, with four molecules of C6H14O2N4HBr · H2O in the unit cell of dimensions a = 11.26 Å, b = 8.65 Å, c = 11.25 Å, and β = 91.5°. The positions of the two bromine atoms in the asymmetric unit were determined from the Patterson projections. A three-dimensional β synthesis based upon these atoms was calculated and this yielded the rest of the structure. The structure was refined by the three-dimensional least-squares method using about 1956 reflections. The final R factor is 0.102. The estimated standard deviations are 0.032 to 0.035 Å in bond lengths and about 2° in bond angles.
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