Abstract
The analysis of neutron-diffraction data collected at room temperature from a single crystal of Rb(H0.45D0.55)2PO4 is shown to require a model of the partially deuterated structure that treats the H and D atoms separately. From the refined structural parameters the length of the symmetric O-(D,D)-O bond in (fully deuterated)RbD2PO4 is estimated as 2.522(4) AA, with a D-site separation of 0.466(8) AA.
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