Abstract
The crystal structure of [(dibenzo-18-crown-6)H3O+](FeCl−4) has been determined by X-ray diffraction and refined to R = 0.06 for 1811 non-zero independent reflections. The oxonium cation is located in the center of the ether cavity. The O(oxonium)⋯O(crown) distances vary from 2.63(1) to 2.73(1) Å. Hydrogen bonding interations of the oxonium ion with two O atoms of the crown and with one Cl atom from FeCl−4 anion are observed.
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