Abstract
Catalyzed by Ir[dF(CF3)ppy]2(dtbbpy)PF6, the coupling of potassium organotrifluoroborates with Baylis–Hillman derivatives under visible light irradiation has been developed. Based on the mechanism of reductive quenching cycle, it provides an easy, mild, efficient method for the synthesis of a variety of α,β-unsaturated carboxylic esters derivatives in a broad scope of the substrates.
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