Abstract

SummaryBrief comparison has been made between the alkaline cyanide and acid citrate gold plating baths. Operating conditions of a proprietary acid bath and their effect on cathode efficiency have been investigated. The low gold and nickel metal content generally adopted in these baths and the marked effect of slight variation in these metals on the characteristics of the deposit and trouble-free running of the process make regular analytical control important, as this affects economy of process and quality of product. Brief mention has been made of the application of atomic absorption spectrophotometry as a convenient means of analytical control. Plating distribution can be greatly improved by careful consideration of anode configuration and cathode jig design. The most suitable anode material was found to be gold strip, or as an alternative, platinized expanded titanium mesh. In the proprietary acid bath under consideration, carbon or stainless steel anodes were found to be unsuitable.

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