Abstract
The observed isotopic effect in CO 2 + H ads reaction showed that at 0.05 V the rate determining step is ▪ formation whereas at 0.2 V the reorientation of adsorbed intermediate: ▪ is probably the slowest step of reaction. The oxidation of adsorbed product is slower in D 2SO 4 than H 2SO 4 solution like the surface oxidation of platinum. The rate determining step of COOH ads oxidation is a reaction with OH ads.
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