Abstract
Approximate homogeneity ranges at about 1073 K have been determined for some (Mg, Me ) 3(PO 4) 2 solid solutions. X-ray powder diffraction data are given and the observed changes in unit cell dimensions are discussed. The Mg 3(PO 4) 2 structure, isotypic with γ-Zn 3(PO 4) 2, contains five- and six-coordinated cation sites, M1 and M2 respectively. The M1 site preference order is Zn 2+ > Co 2+ > Fe 2+ > Mg 2+ > Mn 2+.
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