Abstract
The reaction of some representative N,N-dimethylanilines with dibromoisocyanuric acid has been investigated. In many cases, mixtures of brominated products were obtained; these mixtures were analysed both by gas-liquid chromatography and by proton magnetic resonance spectroscopy. With excess of reagent, perbromination was readily achieved. ��� Significant solvent shifts [δ(CDCl3)-δ(C6D6)] were observed for a wide variety of bromo-N,N-dimethylanilines. This solvent shift phenomenon was used not only for the assignment of structure to reaction products but also for the quantitative analysis of mixtures of bromo-N,N-dimethylanilines.
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