Abstract
Several hexachlorozirconates (M 2ZrCl 6, M = NH 4, Rb and Cs) have been prepared and allowed to react with liquid ammonia. The ammonolysis resembles that of zirconium(IV) chloride in that the ammonobasic zirconium(IV) chloride ZrCl 3( NH 2· xNH 3 is formed, but the enhanced solubility of the product when made from diammonium hexachlorozirconate is considered to result from complex formation. The tensimetric results suggest the initial formation of complex salts M 2[ZrCl 5(NH 2)].
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