Abstract
Abstract Natural lead dioxide samples (β modification) from Cap Garonne, Mine du Pradet, France and Mount Trevasco, Italy were studied by single crystal X-ray and electron diffraction, clearly manifesting the rutile-type structure. A needle from the Mount Trevasco sample was investigated on a single crystal diffractometer: P42/mnm, a = 495.81(10), c = 338.66(7) pm, wR = 0.0513, 117 F 2 values (all data) and nine variables (293 K data). An additional data set at T = 90 K gave no hint for structural distortions.
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