Abstract
The tetranuclear cluster rhenium complexes Cs3H[Re4Q4Cl12] · 3.33H2O (Q = Te (I) and Se (II)) with the Cl atoms as terminal ligands were obtained and structurally characterized. The structures of complexes I and II were determined by X-ray diffraction analysis. Their isostructural crystals are monoclinic; space group C2, Z = 6; a = 26.403(8) A, b = 16.495(5) A, c = 11.744(3) A, β = 91.25(2)°, V = 5113(2) A3 (I); a = 26.573(3) A, b = 16.461(3) A, c = 11.726(2) A, β = 91.381(4)°, V = 5127.6(14) A3 (II).
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