Abstract
AbstractPhosphate esters play important roles as biological active principles and synthons in chemistry. An efficient metal‐free approach for the synthesis of phosphate esters through sp3 CH activation is described. By using tetrabutylammonium iodide (Bu4NI) as a catalyst and tert‐butyl hydroperoxide (TBHP) as an oxidant, various toluene derivatives and phosphorus nucleophiles are tolerated in this transformation, affording the corresponding products in moderate to good yields.magnified image
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