Abstract
The reaction of 2,2 ′-di(hydroxymethyl)biphenyl with ( t-Bu) 3Al leads to the formation of the bimetallic compound [( t-Bu) 4Al 2(HOCH 2C 12H 8CH 2O) 2] ( 1) with two hydroxyl groups. The compound 1 has been characterized by 1H and 13C NMR spectroscopy, cryoscopic molecular weight measurements and elemental analysis and molecular structure has been confirmed by X-ray crystallography. The 18 membered cycle (Al 2O 4C 12) of 1 adopts a configuration with endocyclic oxygen atoms that allow for the intra-molecular hydrogen bonding formation.
Published Version
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