Abstract
Abstract The reaction of 2,6-diformyl-4-methylphenol, triethylenetetramine, and copper(II) perchlorate hexahydrate in the 2:2:4 molar ratio formed a macrocyclic tetracopper(II) complex [Cu4(L)(OH)2](ClO4)4 where H2L denotes the macrocycle formed by two molecules of 2,6-diformyl-4-methylphenol and two molecules of triethylenetetramine. The two hydroxide groups, each bridging a pair of copper(II) ions, are facing each other in a close distance so as to be replaced by an azide ion, affording [Cu4(L)(N3)](ClO4)5.
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