Abstract

Summary The temper embrittlement affecting the HAZ of 2 1/4Cr-1Mo steel subjected to SR treatment and subsequent reheating is investigated with synthetic HAZ specimens and compared with the embrittlement observed in specimens tempered in the same temperature range without SR treatment (direct tempering). The synthetic HAZ specimens are de-embrittled on application of suitable SR treatment (975 K × 5 hours). Subsequent reheating at 775 to 925 K, however, produces four different types of embrittlement in the specimens. These are the second, third, fourth, and fifth types of embrittlement already identified in the direct-tempered specimens. The first type of embrittlement which occurs during direct tempering in the shortest time range does not appear after SR treatment. The second type (the short-term type), which occurs over a wide time-temperature range during direct tempering, only appears in a narrow range after SR treatment. The third and fourth types (the long-term types) occur just as intensively as during direct tempering. The fifth type (the high-temperature type) also appears after SR treatment. This suggests that embrittlement in the short-term range is to some extent suppressed by SR treatment, but the types of embrittlement arising in the long-term range and high-temperature range occur after SR treatment as well. The ‘step cooling process’ can be applied for short-term detection of temper embrittlement in this steel. However, there is considered to be little or no embrittlement promotion effect due to step cooling per se.

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