Abstract
Crystals of 15 rare-earth element phosphates, which provide a set of standard reference samples in X-ray electron probe microanalysis, were synthesized and tested for homogeneity and stoichiometry. The phosphates were synthesized in two stages, the preparation of aqueous phosphates and crystal growth in a solution of potassium polymolybdate K2Mo3O10. The tests of the synthesized crystals confirmed their reliability as reference samples.
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