Abstract

Reactions of cycloalkanone enamines with H 2 O 2 gave bis(1-morpholinocyclopent-1-yl)- and bis(1-morpholinocyclohex-1-yl)-peroxides, which were studied by NMR spectroscopy and X-ray diffraction. Thermolysis of bis(1-morpholinocyclohex-1-yl)-peroxide in n -hexane resulted in two major products, viz. , cyclohexanone and morpholine.

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