Abstract
Two new vanadium(III) phosphates have been synthesized hydrothermally and characterized structurally by Rietveld refinement of X-ray powder diffraction data. The first, VPO 4 .H 2 O, is monoclinic with a=6.6953(2) A, b=7.7925(3) A, c=7.3504(2) A, and β=115.255(1) o . The structure was refined in space group C2/c (No. 15). The compound is isostructural with one form of NiSO 4 .H 2 O and MnPO 4 .H 2 O and closely related to a large class of hydrated divalent metal sulfates with the structure of the mineral kiesserite, MgSO 4 0.H 2 O
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