Abstract
A new co-crystallized complex [Me2NH2]6[VIV12VV6O42][VON(CH2CH2O)3]·2H2O (1) based on mixed valence polyoxovanadate [VIV12VV6O42]6− and a new mononuclear vanadium complex [VON(CH2CH2O)3] (2) were synthesized by controlling conditions of solvothermal synthesis and characterized by single crystal XRD, IR, XPS and EA, respectively. The compound 1 presents interesting antiferromagnetic interaction in solid state and luminescent property in aqueous solution.
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