Abstract
A 3D MOF {[Ni(H2O)6][Ni4L2(μ3-OH)2(H2O)2]}n (1) with a (4,8)-connected flu net is constructed by a butterfly-like tetranuclear [Ni4(μ3-OH)2(COO)8]2− anionic cluster and organic linker 2,3′,5,5′-biphenyl tetracarboxylic acid (H4L). The disordered [Ni(H2O)6]2+ cations fill in the free voids of anionic framework in 1. Magnetic susceptibility measurements indicate that complex 1 shows weak antiferromagnetic interactions.
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