Synthesis of tris[2-(2-furyl)ethyl]phosphine its chalcogenides and Pdii complex

Alexander V Artem’Ev,Nina K Gusarova,Anastasiya O Sutyrina,Yurii V Gatilov,Boris A Trofimov

doi:10.1016/j.mencom.2016.07.016

Synthesis of tris[2-(2-furyl)ethyl]phosphine its chalcogenides and Pdii complex

Alexander V Artem’Ev, Nina K Gusarova + Show 3 more

https://doi.org/10.1016/j.mencom.2016.07.016

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Journal: Mendeleev Communications	Publication Date: Jul 1, 2016
Citations: 5

Affiliation: A.E. Favorsky Irkutsk Institute of Chemistry, Novosibirsk Institute of Organic Chemistry, Novosibirsk State University

#Synthesis Of Tris #Complex Of Trans + Show 5 more

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Abstract

Nucleophilic addition of PH3 to 2-vinylfuran in the KOH/DMSO(H2O) suspension affords 65% of tris[2-(2-furyl)ethyl]-phosphine, whose treatment with H2O2, Se or PdCl gives the corresponding phosphine oxide, selenide and complex of trans-[Pd(L)2Cl2] type in good to excellent yields.

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