Abstract
An unproblematic determination of the structure of the pseudooxide TiNF, a light green to olive green, air stable and chemically substantially inert powder, has been achieved by synchroton‐powder diffraction. TiNF has an anatase structure and does not exhibit any superstructure, even according to electron‐microscopic findings. TiNF was synthesized by ammonolysis of activated (NH4)2TiF6 with a stream of dry, O2‐free NH3.
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