Abstract
In this work, CZTSe was synthesized by direct fusion of chemical elements in a quartz ampoule. XRD method was ineffective for evaluating the single-phase nature of the product, due to overlapping characteristic CZTSe peaks with peaks of secondary phases. While Raman spectroscopy revealed the presence of phases like Cu2SnSe3, ZnSe and SnSe in the sample. By recrystallization in a melt-solution of alkali metal salts at a temperature of 750° C, a single-phase product was obtained. As a solvent, a KI-KCl eutectic mixture was selected. According to the results of Raman spectroscopy and SEM, it was shown that after recrystallization in a melt-solution for 14 hours, single-phase and homogeneous composition of CZTSe is achieved.
Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callMore From: BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
