Abstract
1. A method has been developed for the preparation of a series of triorganosilylmethyl esters of diphenylphosphoric acid. 2. All the triorganosilylmethyl esters of diphenylphosphoric acid which were examined undergo thermal rearrangement involving the migration of a radical from the Si atom to the methylene C atom according to a 1,2-shift. The influence of the type of radical at the Si atom on the rate of the rearrangement has been studied.
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