Abstract
A convenient method for the synthesis of Ru(II) pyridoxal thiosemicarbazone complex has been described. Elemental analysis, spectral methods and single crystal X-ray diffraction analysis were used to confirm the composition of the complex. The synthesized complex could act as an efficient, reusable homogeneous catalyst for transformation of aldehydes to the corresponding primary amides in the presence of NH2OH·HCl. The effect of solvent, base, temperature, time, catalyst loading and recyclability was also investigated.
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