Abstract
An effective and atom‐economic synthesis of quinolino[3′,4′:4,5]pyrrolo[1,2‐f]phenanthridines has been developed. The protocol involves a site‐selective Sonogashira reaction of 3,4‐dihaloquinoline, followed by a domino C–N coupling/hydroamination/C–H arylation reaction. Quinolino[3′,4′:4,5]pyrrolo[1,2‐f]phenanthridines represent a hitherto unknown class of heterocyclic compounds.
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