Abstract
Condensation of 2-methyl-(3,4,6-tri- O-acetyl-1,2-dideoxy-α- d-glucopyrano)-[2′,1′:4,5]-2-oxazoline with p-nitrophenyl 2,3-di- O-acetyl-β- d-galactopyranoside ( 4), followed by saponification of the resulting disaccharide derivative, produced p-nitrophenyl 6- O-(2-acetamido-2-deoxy-β- d-glucopyranosyl)-β- d-galactopyranoside as a crystalline compound. Reaction of 2-methyl-[4,6-di- O-acetyl-1,2-dideoxy-3- O-(2,3,4,6-tetra- O-acetyl-β- d-galactopyranosyl)-α- d-glucopyrano]-[2′,1′:4,5]-2- oxazoline with 4 in a similar reaction-sequence provided the title trisaccharide compound.
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