Abstract
Efficient syntheses of 1,3,4-thiadiazoles and bis-thiadiazoles by the reaction of hydrazonoyl halides with carbonothioic dihydrazide are reported. In addition, 1,2,4-triazolo[3,4- b][1,3,4]thiadiazole is obtained via oxidative cyclization of bis-(substituted methylene)carbonothioic dihydrazone.
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