Abstract
AbstractThe development of efficient methods for the combinatorial synthesis of N‐glycosyl conjugates is vital for many fields of modern synthetic organic chemistry. Herein, we report a multicomponent domino process for the regioselective synthesis of a large array N‐glycosyl‐Asp‐urea conjugates, which could be further functionalized in a chemoselective way, starting from easily accessible reactants such as N‐glycosylamines, fumaric acid monoesters, azides, and isocyanates. The process occurs under very mild conditions, does not require the use of strong bases/acids or high temperature, and is highly versatile, working efficiently with a range of protecting groups and substituents.
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