Abstract
A series of new carboranyl organosilicon monomers have the potential to be used as high temperature oils, as building blocks in sol-gel processes and as an additive in composites. The versatile and easy preparation of the four polyhedral carboranyl derivatives are based on UV initiated hydrothiolation. The compounds were isolated in good yields (65–95%) and characterized by 1H, 11B, 13C and 29Si NMR, IR spectroscopy, HRMS ESI and elemental microanalysis. Assignment of 1H and 13C NMR spectra was made on the basis of 2D experiments of COSY, HMQC and HMBC.
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