Abstract
A number of earlier unknown tri- and tetranuclear organometallic clusters of group VIII transition metals was synthesized by the addition of coordinatively unsaturated species to a single metal-metal bond. A number of novel heteronuclear clusters, CpCp 2 ′ Rhm2(μ−CO)3(μ3−CO), (Cp′=Cp, Cp*; M2=Ru2, Fe2; RuFe); Cp2Cp 2 * Rh2M2(μ3−CO)3 (M = Ru, Fe); , Cp3Cp*Rh3M(μ3−CO)2(μ3−d) (M = Ru, Fe); Cp2Cp 2 *> Rh2Co2(μ3−CO)2,etc., was obtained.
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