Abstract
Nanostructured MgO powders have been synthesized using chemical methods. Ammonium oxalate and Magnesium sulphate were used as the precursor materials. The weight ratios of the raw materials (ammonium oxalate/Magnesium sulphate) were 0.9, 1, 1.1, 1.2, 1.3, and 1.4. As a result of chemical reaction (between them), Magnesium oxalate was synthesized. Produced samples were analyzed by XRD and SEM. The results show that the best ratio (for ammonium oxalate/Magnesium sulphate) is 1.4. Produced Magnesium oxalate powder was heated at 450 and 550°C. The final product was MgO nanopowder. XRD studies indicate that the highest ratio of MgO was observed in the specimen heated at 450°C.
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