Abstract
Transsilylation of N-methyl-N-trimethylsilylacetamide with chloromethyl(dimethyl)silylnitrate ClCH2SiMe2ONO2 led to the formation of (N-acetyl-N-methyl)aminomethyl](dimethyl)silyl nitrate, the (O–Si)-chelate with the intramolecular coordination C=O→Si bond. Spectral characteristics of this compound and the reaction product of N-[chloro(dimethyl)silylmethyl]-N-methylacetamide with silver nitrate are identical.
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