Abstract
(+)-Goniothalamin has been synthesized by lipase catalyzed resolution of (1 E)-1-phenylhexa-1,5-dien-3-ol using vinyl acrylate as acyl donor followed by ring closing metathesis of the formed (1 R)-1-[( E)-2-phenylvinyl]but-3-enyl acrylate. The unreacted alcohol from the resolution, (1 E,3 S)-1-phenylhexa-1,5-dien-3-ol, was esterified non-enzymatically, and used for synthesis of (−)-goniothalamin.
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