Abstract
In this study, the first magnetite nanoparticles (Fe3O4), and MIL-100(Fe) nanocatalyst via in situ two-step hydrothermal strategies were synthesized in which Fe3O4 is known as the magnetic core. MIL-100 (Fe) grows as a shell at the Fe3O4 level and adjusts the shell thickness by precisely controlling the reaction time from 37.10 to 45.95 nm. The structural, morphological, magnetically, optical, and chemical bonding studies; XRD, FESEM, TEM, VSM, UV-Vis, and FTIR measurements were carried out. The results of the above analyses demonstrated core-shell structure is formed. The catalyst synthesized in the degradation of methylene blue was investigated as a heavy organic compound.
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