Abstract

The dihydrochalcones phloretin and phloridzin are major phenolic constituents of apple fruit. Phloretin-d4, deuterated at both the α and β positions, was prepared by hydrogenolysis of naringenin and by deuterium exchange from unlabelled phloretin using Pd/C and sodium formate with methanol-d1 as the source of deuterium. Deuterated derivatives of the glycosides, phloridzin and naringin dihydrochalcone, were similarly prepared. Copyright © 2006 John Wiley & Sons, Ltd.

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