Abstract
The compounds [ Fe(dppe)(CO)(CNR)(RNCNRC NR)] (IIa: R = Ph, IIb; R = p-tol= 4-methylphenyl) have been prepared by reaction of [Fe(dppe)(CNR) 4]-(ClO 4) 2 with KOH. The structure of IIb has been determined by X-ray diffraction IIb can be protonated in two steps with HClO 4 to give the cationic complex species { Fe(dppe)(CO)(CNPh)[PhNCNPhC (NHPh)]} [ClO 4] and trans-{Fe(dppe)-(CO)(CNPh) 2[C(CNHPh) 2][ClO 4]
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