Abstract
A procedure for the synthesis of borosiloxane compounds by the reaction of polydimethylsiloxane with boric acid upon heating in a cylindrical reaction vessel is presented. The mixing of the reaction components in the considered method occurs spontaneously due to the sublimation of boric acid vapor and its movement in a natural way from the lower part of the reaction vessel to the upper part through the volume of polydimethylsiloxane. The technique makes it possible to synthesize borosiloxane compounds without the use of special equipment, increased energy consumption, and chemical solvents.
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