Abstract
Using o-dihydroxybenzene and 1,11-dichloro-3,6,9-trioxaundecane as raw materials,sodium hydroxide as template,DMF as solvent and appropriate amount of 2,6-di-tert-butyl-4-methylphenol as antioxidant,benzo-15-crown-5 was successfully synthesized under ultrasonication at temperature 60~70 ℃.Compared with traditional synthetic routes,reaction time could be reduced to within 2 h,and the yield reached up to 30.7%.
Full Text 
Sign-in/Register to access full text options
Sign-in/Register to access full text options 
Published version (
Free)
Free) 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a call
