Abstract
The thionation of a protected uridine with the aid of P2S5 has given the corresponding 4-thiouridine derivatives, which have been phosphorylated at the 5′ or the 2′(3′)hydroxyl. On being heated in aqueous pyridine solution with liquid hydrogen sulfide, cytidine phosphates also form 4-thiouridine phosphates. 4-Thiouridine 2′,3′-cyclophosphate has been obtained.
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