Abstract

Heating ortho-manganated aromatic ketones and RNCO (R = Et, n-Pr, p-tolyl) in dioxane for 3 – 7 h leads to production of 3-alkylidene phthalimidines. The alkylidene phthalimidines derived from aliphatic isocyanates were unstable and were reduced to phthalimidines prior to purification and characterization.

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