Abstract
2-Deoxy-β-D-ribose 1-phosphate (1) was synthesized in a stereoselective manner and isolated with no detectable contamination by its α-isomer (4). Explicit configuration of 4 was first determined by NMR comparison with 1 judging from NOE results and their coupling constants. Natural purine nucleoside phosphorylase (PNPase) did not recognize 1 and gave no products such as α- or β-deoxynucleosides.
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