Abstract
AbstractMonopalmitin, mono‐olein, and monostearin have been synthesized in quantities of up to 100 grams with recoveries ranging from. 80%‐85%. The monoglycerides were reacted with a 0.5 molar excess of pyridine and fatty acid chloride to produce 1, 3,‐diglycerides. The recoveries ranged from 60%‐70% and, in addition, considerable amounts of triglyceride were obtained from this reaction. Partial glycerides were converted to 100‐gram batches of triglyceride in a similar manner with recoveries ranging from 80%‐90%. Purification of the partial glycerides was achieved by crystallization. In addition to this technique, certain triglycerides were purified by elution through a column of alumina. Purity of the glycerides, as determined by TLC, G‐LC, and pancreatic lipolysis, was estimated to be at least 99%.
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