Abstract
Two new oxidoperoxidocompounds with isonicotinic acid N-oxide have been obtained and characterized. Both compounds are oxidodiperoxidomolybdates built with the same isonicotinic acid N-oxide moiety, first one – potassium salt: K(C6H4MoNO8)H2O (denoted as K-isoO) and the ammonium salt: (NH4)2(C6H4MoNO8)22H2O (NH4-isoO). They were investigated using powder X-ray diffraction (K-isoO) or single crystal (NH4-isoO) techniques. In addition, they were examined with the use of XRPD versus temperature method, IR spectroscopy and catalytic activity studies. This work is also a continuation of our previous papers and presents a summary of studies of peroxidomolybdates forming inorganic–organic hybrids with pyridine carboxylic acids.
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