Abstract
Crystals of a sodium barium orthoarsenate (V) nonahydrate were synthesized by slow evaporation from aqueous solutions. The crystal structure was solved and refined by single-crystal X-ray diffraction. The crystal is cubic, space group P213, a=10.838(2)Å; Z=4 and V=1273.1(2)Å3. Its structure is composed of BaO9 and NaO6 polyhedra and AsO4 tetrahedral units. The short hydrogen bond length O4H42⋯O2B of 2.496Å was confirmed by infrared spectroscopy. In addition, Raman spectrum was recorded in order to study the arsenate group and the cation motion (lattice modes) in the title compound.
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