Abstract
A new 3D porous zinc phosphonate, Zn 6(HL) 4 · 6H 2O 1 (H 4L = C 6H 11N(CH 2PO 3H 2) 2) has been synthesized by hydrothermal reaction at 180 °C and structurally characterized by X-ray diffraction as well as by infrared spectroscopy, elemental and thermogravimetric analysis. The structure of compound 1 features a 3D open-framework built from ZnO 4 tetrahedra linked together by bridging phosphonate groups. Each zinc cation is tetrahedrally coordinated by four phosphonate oxygen atoms from four ligands, each of which connects with six zinc atoms, resulting in channel systems of different size.
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